Investigating Unknown Material Collected In The Field

ufos-scientificresearch |  The Journal "Progress in Aerospace Sciences" is an "...invitation only international review journal, designed to be of broad interest and use to all those concerned with research in aerospace sciences and their applications in research establishments, industry and universities." 

Volume 128, January 2022 contains an article by authors Garry P. Nolan, Jacques F. Vallee, Sizun Jiang, and Larry G. Lemke. Its title is "Improved instrumental techniques including isotopic analysis, applicable to the characterization of unusual materials with potential relevance to aerospace forensics." The article was made available on line on 9 December 2021. Many thanks to researcher Jonathan Davies for pointing me to this article. 

Contents

The introduction spells out that precisely identifying unknown material is an issue, in a number of areas, e.g. medicine, space exploration, and military intelligence. 

The first section of the article reviews analytical processes which are currently in use, e.g. mass spectrometry and x-ray spectroscopy. The second section "Basic approaches for the initial characterization of unknown materials" reports on the material analysis using Inductively Coupled Plasma Mass Spectrometry (ICP-MS) and Secondary Ion Mass Spectrometry (SIMS.) These determine the masses of atomic components of the material. Other analytical processes are also discussed. 

Council Bluffs, Iowa, a case study

Section 3 "Investigating unknown material collected in the field: A Case Study" concerns an incident on the 17 December 1977, which occurred in Council Bluffs, Iowa. At 1945 CST "...a red, luminous mass was observed by two Council Bluffs residents, as it fell to Earth near the northern city limits..." At the scene the witnesses found an area "...covered by molten metal that glowed red-orange, igniting the grass. Police and fire brigade personnel who attended the scene within 15 minutes all saw the mass, estimated at 35-55 pounds. An investigation was conducted with three initial thoughts in mind. These were, an industrial accident, an aeronautical malfunction or a meteorite (despite there being no cratering.)  After investigations, it was concluded that it was not re-entering space debris; not falling material from an aircraft, not a meteorite, nor was it a hoax.  It was also noted that two witnesses of the eleven witnesses, described a round object hovering in the sky, edged by red blinking lights. 

The retrieved material had three components, namely "solid metal, slag and white ash inclusions in the slag." Vallee provided a piece of the original material for further testing. "...our initial conclusion was that sample components were consistent with a terrestrial origin." A recently developed Multiplexed Ion Beam Imaging" (MIBI) instrument was used which is capable of measuring a broader range of isotopes. Using this instrument investigators concluded that "All isotopic ratios were similar between the samples and did not show any statistically significant deviations from expected terrestrial normal except for 57Fe..." However, there was a suggested conventional explanation for this 57Fe deviation.

Speculative conclusions

Section 5, "Speculative conclusions" includes the statement:

"Our experience with the Council Bluffs case study shows how difficult such a determination can be, even when abundant evidence is collected within minutes of an event, supported by reliable testimony from multiple witnesses and in well-defined meteorological conditions."

The authors speculate about the hovering, round object edged with red lights;  that "Such an object might have ejected the mass of material observed by the other witnesses and recovered by police." They note that "The materials from Council Bluff show no evidence suggesting it was (sic) been engineered or designed. The material would not be expected to form naturally, and has been shown does have unusual inhomogeneity."